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id="azbi334" class="proBig"><div id="nmtacjl" class="bigimg"><div><p class="pic"><img src="https://tyunfile.71360.com/WaterMark/UploadFile/shlinchen/637278336263828125/6823745.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div><div id="uoqxegi" class="smallimg"><div><p class="pic"><img src="https://tyunfile.71360.com/WaterMark/UploadFile/shlinchen/637278336263828125/6823745.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="g3qik79" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價格要求：</span>面議</p><p><span>所在地：</span>上海市</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產品關鍵詞：</span>穩(wěn)定供應泛解酸內酯銷售,泛解酸內酯</p><p><span>***更新：</span>2020-07-02 00:34:22</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="ig8qszb" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">上海臨辰醫(yī)藥科技有限公司</a></p><p><span>聯(lián)系人：</span>葉海岑</p><p><span>郵箱: </span>info@linchenpharm.com</p><p><span>電話: </span>13761181955</p><p><span>傳真: </span>021_</p><p><span>網址: </span></p><p><span>手機: </span>021-31606595</p><p><span>地址: </span>辰花路5088弄221號</p><p>[當前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="dhzbiu7" class="page-proshow02"><p class="title">詳細說明</p><div id="82qskce" class="box"><p><p> 生產工藝為：D-泛解酸鈉溶液 –內酯化，得到D-泛解酸內酯溶液-溶液減壓濃縮脫除水分-結晶-固液分離，母液回套至減壓濃縮脫水-D-泛解酸內酯成品-β-丙氨酸、氧化鈣、甲醇進行鈣化反應，生成β-丙氨酸鈣-加入甲醇、D-泛解酸內酯進行酰化反應，生成D-泛酸鈣-結晶、離心- D-泛酸鈣濕粉干燥-整粒、包裝入庫。 </p> <p> <br /> </p> <p> 一種高純度的D?泛酸內酯的合成方法包括步驟:將DL?泛酸內酯加入到水中,在pH為6.0?8，穩(wěn)定供應泛解酸內酯銷售.0用酶水解，穩(wěn)定供應泛解酸內酯銷售,得到D?泛解酸以及L?泛酸內酯;將上述水溶液經有機溶劑萃取，穩(wěn)定供應泛解酸內酯銷售,得到D?泛解酸的水溶液以及L?泛酸內酯有機溶液。 D-泛解酸內酯是一種重要的原料藥中間體。穩(wěn)定供應泛解酸內酯銷售</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="穩(wěn)定供應泛解酸內酯銷售,泛解酸內酯" src="https://tyunfile.71360.com/WaterMark/UploadFile/shlinchen/637278336263828125/6823745.png"></div><p style="text-indent:25px">一種ＤＬ－泛酰內酯的拆分方法?，F(xiàn)有拆分方法中使用的拆分劑在拆分ＤＬ－泛酰內酯時的選擇性低，使ＤＬ－泛酰內酯的總利用率低，提高了拆分ＤＬ－泛酰內酯的生產成本。本發(fā)明所用的拆分劑為有機堿Ｒ－ＮＨ＃－［２］，其中Ｒ為Ｃ＃－［１５］Ｈ＃－［１５］，包括以下步驟：ａ）用純化后的拆分劑與酸反應，加水、加熱溶解，滴加ＤＬ－泛酰內酯水解液，拆分劑：ＤＬ－泛酰內酯的摩爾比＝０．５－０．７∶１；ｂ）抽濾由ａ得到的反應液，濾餅進行消旋、回收拆分劑處理，濾液加入有機溶劑進行共沸脫水，蒸去過量有機溶劑進行結晶。本發(fā)明明顯提高了拆分劑對Ｄ－泛酰內酯的選擇性，提高ＤＬ－泛酰內酯的總利用率，拆分收率高，減少拆分劑的用量且容易重復回收利用，降低拆分ＤＬ－泛酰內酯的生產成本。穩(wěn)定供應泛解酸內酯銷售作為腦代謝的D-泛解酸內酯，主要用于生產泛酸鈣。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="穩(wěn)定供應泛解酸內酯銷售,泛解酸內酯" src="https://tyunfile.71360.com/WaterMark/UploadFile//637280289509208985/415071.png"></div><p style="text-indent:25px">水解酶催化選擇性拆分制備D-泛解酸內酯DL-泛解酸內酯可經手性拆分得到所需要的D-泛解酸內酯。化學法拆分所需的化學拆分劑或結晶操作一般較為昂貴，而利用水解酶催化的動力學拆分，具有節(jié)能環(huán)保、產品光學純度高等優(yōu)點，更適用于工業(yè)生產。水解酶選擇性水解泛解酸內酯，根據(jù)選擇性可分為L-泛解酸內酯水解酶和D-泛解酸內酯水解酶。DL-泛解酸內酯經L-泛解酸內酯水解酶水解，留下D-泛解酸內酯，產生的L-泛解酸再經化學內酯、外消旋轉為DL-泛解酸內酯。已知的L-泛解酸內酯水解酶，大多來源于細菌，如多形無色桿菌、蘇云金芽孢桿菌、放射性土壤桿菌、根*農桿菌。</p><p> SHIMIZU S 等進一步研究發(fā)現(xiàn)一株紅串紅球菌可以直接完成該氧化還原過程，說明紅串紅球菌自身不僅可以產L-泛解酸內酯脫氫酶，還可以產還原過程所需的酮泛解酸內酯還原酶。同時他們還提出酮泛解酸內酯在中性pH 條件下會發(fā)生自發(fā)水解形成酮泛解酸，酮泛解酸再經過大腸 </p> <p> 桿菌中酮泛解酸還原酶催化形成D-泛解酸，而后在酸性條件下閉環(huán)成D-泛解酸內酯，這就解釋了1973 年發(fā)現(xiàn)酮泛解酸還原酶延滯2.2 min起作用的原因。 </p> <p> <br /> </p> <p> D-泛解酸內酯是合成D-泛酸的重要中間體。 </p> <p> <br /> 采用異丁醛、甲醛和**為原料經過化學合成獲得DL-泛解酸內酯。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="穩(wěn)定供應泛解酸內酯銷售,泛解酸內酯" src="https://tyunfile.71360.com/WaterMark/UploadFile/shlinchen/637278338760781250/415124.png"></div><p> 微生物選擇性的不對稱水解DL-泛解酸內酯中的D-泛解酸內酯，得到D-泛解酸，再將D-泛解酸進行內酯化生產D-泛解酸內酯。該方法工藝控制簡單，微生物酶專一性好，可以得到高光學純度的D-泛解酸內酯。 </p> <p> <br /> </p> <p> <br /> </p> <p> <br /> </p> <p> 利用D-泛解酸內酯水解酶N末端序列,并根據(jù)NCBI中公布的D-泛解酸內酯水解酶cDNA序列設計了一個特異引物,該引物結合Oligo(dT)15,以串珠鐮孢霉(Fusarium moniliforme)CGMCC 0536 mRNA反轉錄得到的總cDNA為模板進行擴增,獲得約1.5kb左右的片段,將其克隆到T載體上進行測序,對測得的序列進行分析,重新設計了一對引物,并在引物兩端分別加上限制酶EcoRI和SalI的識別位點序列,利用熱啟動PCR成功地擴增出了D-泛解酸內酯水解酶基因, 用微生物酶將 D, L-泛解酸內酯拆分得到 D-泛解酸內酯，與 B再一丙氨酸鈣縮合生產 D-泛酸鈣。高純度泛解酸內酯生產</p><p style="text-indent:25px">D-泛解酸內酯是合成D-泛酸的重要中間體。穩(wěn)定供應泛解酸內酯銷售</p><p> 以水和甲苯為溶劑體系，通過添加D-泛解酸內酯作為晶種，誘導結晶獲得D-泛解酸內酯的方法。 </p> <p> <br /> </p> <p> 但本法在生產過程中用了甲苯，生產過程VOC排放較高，且通過誘導結晶獲得的一次收率較低，產品比旋度較低。 </p> <p> <br /> </p> <p> D-泛解酸內酯的工業(yè)制備是由DL-泛解酸內酯拆分而來的。 </p> <p> <br /> </p> <p> 作為一種重要的醫(yī)藥中間體，主要用于合成維生素類藥D-泛醇及神經營養(yǎng)藥D-泛酸鈣。 </p> <p> <br /> </p> <p> D-泛酸鈣是維生素B5，作為重要的營養(yǎng)成分，***用于飼料添加劑、食品添加劑、醫(yī)藥等領域； </p> <p> <br /> </p> <p> D-泛醇是維生素原B5，***用于護發(fā)用品和化妝品中。 </p> <p> <br /> 穩(wěn)定供應泛解酸內酯銷售</p><p style="text-indent:25px">上海臨辰醫(yī)藥科技有限公司坐落辰花路5088弄221號，交通便利，環(huán)境優(yōu)美，是一家貿易型企業(yè)。公司致力于為客戶提供安全、質量有保障的質量產品及服務，是一家私營有限責任公司企業(yè)。以滿足顧客要求為己任；以顧客永遠滿意為標準；以保持行業(yè)**為目標，提供***的[ "泛解酸內酯", "有機可可粉有機果粉", "阿拉伯膠瓜爾膠 ", "BIS TRIS " ]。上海臨辰醫(yī)藥將以真誠的服務、創(chuàng)新的理念、***的產品，為彼此贏得全新的未來！</p></p><br /><p>文章來源地址: http://m.cdcfah.com/cp/463432.html</p></div></div></div></div></div><div id="yh7wdfm" class="page-right twoColRt"><div id="8lce84v" class="box01 margin10 clearfix"><h3><a href="http://m.cdcfah.com/cp/">猜你喜歡</a></h3><div id="8lx38tp" class="recomPic likePro"><a href="http://m.cdcfah.com/cp/814588.html"><div><img src="http://tyunfile.71360.com/UpLoadFile/2019/11/1/14/637082168864691056_lgpj_5374157.jpg" alt="福建ZF配件哪家強信息推薦自業(yè)物資供應" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></div><p>福建ZF配件哪家強信息推薦自業(yè)物資供應</p></a></div><div id="zofh2kb" class="recomPic likePro"><a href="http://m.cdcfah.com/cp/846569.html"><div><img 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