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src="https://tyunfile.71360.com/UploadFile/shbeicanghuagong/637326786820351562/866617.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div><div id="73axegk" class="smallimg"><div><p class="pic"><img src="https://tyunfile.71360.com/UploadFile/shbeicanghuagong/637326786820351562/866617.png" class="vcenter" onerror="javascript:this.src='/static/new_net_01/images/nopic.jpg';"></p></div></div></div><div id="ztl3wcb" class="content"><p><span>需求數(shù)量：</span>0</p><p><span>價(jià)格要求：</span>面議</p><p><span>所在地：</span>上海市</p><p><span>包裝要求：</span><span style="color: #f30;"></span></p><p><span>產(chǎn)品關(guān)鍵詞：</span>浙江批量生產(chǎn)β-煙酰胺單核苷酸,煙酰胺單核苷酸</p><p><span>***更新：</span>2020-12-02 03:17:08</p><p><span id="click" >瀏覽次數(shù)：0次</span></p><a rel="nofollow" class="button">聯(lián)系我們</a></div></div><div id="tia33mj" class="rightbox"><h3>公司基本資料信息</h3><p style="border:0;"><a rel="nofollow">上海北倉化工科技有限公司</a></p><p><span>聯(lián)系人：</span>王金良</p><p><span>郵箱: </span>shbeicang@vip.126.com</p><p><span>電話: </span>18516286991</p><p><span>傳真: </span>021_</p><p><span>網(wǎng)址: </span>http://www.shbeicang.cn</p><p><span>手機(jī): </span>021-60459206</p><p><span>地址: </span>金山大道4168號(hào)</p><p>[當(dāng)前離線] <a rel="nofollow"> [加為商友] </a><a rel="nofollow"> [發(fā)送信件] </a></p></div></div><div id="f2kchg8" class="page-proshow02"><p class="title">詳細(xì)說明</p><div id="3ea7bnr" class="box"><p><p style="text-indent:25px">β-煙酰胺單核苷酸鑒別方法： 1.取本品約0. lg ，加水5m l溶解后，加氫氧化鈉試液5ml，緩緩加熱，產(chǎn)生的氨氣使?jié)駶?rùn)的紅色石蕊試紙變藍(lán)（與煙酸的區(qū)別）。繼續(xù)加熱至氨臭完全除去，放冷，加酚酞指示液1?2 滴，用稀硫酸中和，加硫酸銅試液2ml，即緩緩析出淡藍(lán)色的沉淀。 2.取本品，加水溶解并稀釋制成每lm l中約含20ug的溶液，浙江批量生產(chǎn)β-煙酰胺單核苷酸，照紫外-可見分光光度法(通則0401)測(cè)定，浙江批量生產(chǎn)β-煙酰胺單核苷酸，在261nm的彼長(zhǎng)處有很大吸收，在245nm的波長(zhǎng)處有較小吸收，浙江批量生產(chǎn)β-煙酰胺單核苷酸，在245nm波長(zhǎng)處的吸光度與261nm波長(zhǎng)處的吸光度的比值應(yīng)為0. 63?0. 67。 3.本品的紅外光吸收?qǐng)D譜應(yīng)與對(duì)照的圖譜一致。β-煙酰胺單核苷酸使用后洗手，禁止在工作場(chǎng)所進(jìn)飲食。浙江批量生產(chǎn)β-煙酰胺單核苷酸</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="浙江批量生產(chǎn)β-煙酰胺單核苷酸,煙酰胺單核苷酸" src="https://tyunfile.71360.com/UploadFile/shbeicanghuagong/637326786820351562/866617.png"></div><p style="text-indent:25px">β-煙酰胺單核苷酸制備：在500ml的四口瓶中加入150ml的磷酸鹽緩沖溶液。一次性加入2g氯化鎂、10g ATP、7g核糖、10g煙酰胺，在35℃保溫?cái)嚢?。檢測(cè)反應(yīng)體系的pH值，并用10％Na2CO3溶液調(diào)pH＝8.0，再加入1gRK酶粉、2gNAMPT酶粉，攪拌溶解。于37℃下，200rpm攪拌反應(yīng)，利用液相色譜-質(zhì)譜聯(lián)用監(jiān)測(cè)反應(yīng)的轉(zhuǎn)化率，經(jīng)過6小時(shí)反應(yīng)后，檢測(cè)ATP已經(jīng)消耗完畢，停止反應(yīng)。通過進(jìn)一步的過濾，HZ-818型大孔樹脂吸附，凍干，乙醇和水重結(jié)晶即可獲得β-煙酰胺單核苷酸-煙酰胺單核苷酸NMN，收率70％。浙江批量生產(chǎn)β-煙酰胺單核苷酸β-煙酰胺單核苷酸作為一種重要的有機(jī)化工原料，在研究等行業(yè)中具有很廣的用途。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="浙江批量生產(chǎn)β-煙酰胺單核苷酸,煙酰胺單核苷酸" src="https://tyunfile.71360.com/UploadFile/shbeicanghuagong/637326786502558593/3761852.png"></div><p style="text-indent:25px">β-煙酰胺單核苷酸包裝方法：按照生產(chǎn)商推薦的方法進(jìn)行包裝，例如：開口鋼桶。安瓿瓶外普通木箱。螺紋口玻璃瓶、鐵蓋壓口玻璃瓶、塑料瓶或金屬桶（罐）外普通木箱等。 β-煙酰胺單核苷酸海洋污染物(是/否)：否。 β-煙酰胺單核苷酸運(yùn)輸注意事項(xiàng)：運(yùn)輸車輛應(yīng)配備相應(yīng)品種和數(shù)量的消防器材及泄漏應(yīng)急處理設(shè)備。嚴(yán)禁與氧化劑、食用化學(xué)品等混裝混運(yùn)。裝運(yùn)該物品的車輛排氣管必須配備阻火裝置。使用槽(罐)車運(yùn)輸時(shí)應(yīng)有接地鏈，槽內(nèi)可設(shè)孔隔板以減少震蕩產(chǎn)生靜電。禁止使用易產(chǎn)生火花的機(jī)械設(shè)備和工具裝卸。夏季建議早晚運(yùn)輸，運(yùn)輸途中應(yīng)防暴曬、雨淋，防高溫。中途停留時(shí)應(yīng)遠(yuǎn)離火種、熱源、高溫區(qū)。公路運(yùn)輸時(shí)要按規(guī)定路線行駛，勿在居民區(qū)和人口稠密區(qū)停留。鐵路運(yùn)輸時(shí)要禁止溜放，嚴(yán)禁用木船、水泥船散裝運(yùn)輸。運(yùn)輸工具上應(yīng)根據(jù)相關(guān)運(yùn)輸要求張貼危險(xiǎn)標(biāo)志、公告。</p><p style="text-indent:25px">β-煙酰胺單核苷酸能激發(fā)隨著老化而逐漸衰弱的線粒體產(chǎn)生能量，補(bǔ)充線粒體的活力，供給機(jī)體新的動(dòng)能。β-煙酰胺單核苷酸可以明顯阻抑衰老引起的新陳代謝下降：如血糖值上升，以及免疫機(jī)能下降，對(duì)2型糖尿病有著奇跡般的***效果。β-煙酰胺單核苷酸還可以有效防止衰老引起的視網(wǎng)膜病變及認(rèn)知能力衰退。zui驚人的是，可使與人類相近的實(shí)驗(yàn)動(dòng)物的壽命延長(zhǎng)高達(dá)31%！服用β-煙酰胺單核苷酸的老年動(dòng)物的體力和爆發(fā)力均超過未服用的同齡動(dòng)物60%以上，甚至超越了青年時(shí)期的水平。β-煙酰胺單核苷酸純度不夠，相對(duì)而言另外不確定的物質(zhì)含量就會(huì)增高。</p><div style="width:100%;text-align: center;"><img style="max-width: 640px; max-height: 320px;" alt="浙江批量生產(chǎn)β-煙酰胺單核苷酸,煙酰胺單核苷酸" src="https://tyunfile.71360.com/UploadFile/shbeicanghuagong/637326786687050781/6503284.png"></div><p style="text-indent:25px">β-煙酰胺單核苷酸。別名：煙酰胺核糖一磷酸酯 | 煙酰胺單核苷酸 | Beta-煙酰胺單核苷酸 | 煙酰胺核苷酸。外觀與性狀：白色粉末；溶解性：易溶于水，幾乎不溶于**；穩(wěn)定性：在建議的貯存條件下是穩(wěn)定的；儲(chǔ)存條件：貯存在陰涼處，容器保持緊閉，儲(chǔ)存在干燥通風(fēng)處建議的貯存溫度：-20°C；安全操作的注意事項(xiàng)：在有粉塵生成的地方,提供合適的排風(fēng)設(shè)備；包裝：1kg一包，自封袋外面有鋁箔袋。目前β-煙酰胺單核苷酸主要有化學(xué)合成和酶法兩種制造方法，現(xiàn)階段以酶法制作為主，但是酶法收率不穩(wěn)定，而且化學(xué)合成法較酶法會(huì)貴一點(diǎn)。β-煙酰胺單核苷酸的收容、清掃方法及所使用的處置材料：小量泄漏：盡量將泄漏液體收集在可密閉的容器中。浙江批量生產(chǎn)β-煙酰胺單核苷酸</p><p style="text-indent:25px">生產(chǎn)β-煙酰胺單核苷酸場(chǎng)所使用防爆型的通風(fēng)系統(tǒng)和設(shè)備。浙江批量生產(chǎn)β-煙酰胺單核苷酸</p><p style="text-indent:25px">β-煙酰胺單核苷酸脫乙?；?制備煙酸乙酯核苷)：-5℃，向步驟a制得的含有煙酸乙酯三乙酰核苷的溶液中滴加乙醇鈉溶液(由17.1g，251mmol乙醇鈉溶于160mL乙醇制得)，滴加過程放熱，控制溫度在0℃以下，約0.5小時(shí)加完，滴加完畢，-5℃攪拌反應(yīng)1小時(shí)以完成反應(yīng)(TLC監(jiān)控至原料和中間體1消失)。反應(yīng)完成，滴加醋酸(15.1g，251mmol)酸化至pH為5～6，以除掉過量乙醇鈉，從而淬滅反應(yīng)。然后慢慢加入1400mL甲基叔丁基醚，-5～5℃攪拌析晶0.5小時(shí)，過濾，濾餅用甲基叔丁基醚洗滌，室溫減壓干燥，得到37.8g煙酸乙酯核苷的三氟甲磺酸鹽(含醋酸鈉)，無需除去醋酸鈉，直接用于下一步。前兩步收率加和的總收率約80％，核磁無明顯有機(jī)雜質(zhì)。浙江批量生產(chǎn)β-煙酰胺單核苷酸</p></p><br /><p>文章來源地址: http://m.cdcfah.com/cp/2228618.html</p></div></div></div></div></div><div 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